Number of lithium-based oxide ceramics in Li-Al-Si-O system were synthesized by solid-state reaction route using Li2CO3, Al2O3, and SiO2. The progress of the reaction was monitored using thermogravimetry. A model-free approach was employed to fit the temperature versus mass loss data. Heat capacities were measured as a function of temperature using differential scanning calorimetry. Variation of lithium/silicon ratio resulted in change in heat capacity and average crystallite size in each compound. © 2012 Akadémiai Kiadó, Budapest, Hungary.

Shiv Govind Singh

Department of Electrical Engineering

L. Ahamad

S.K. Rakshit

S.C. Parida

Y.P. Naik

G.A. Rama Rao

S.G. Kulkarni

S.C. Gadkari

Indian Institute of Technology Hyderabad (IITH) is a premier institute of science and technology established in 2008. IITH has been consistently ranked in the&nbsp;<a href="https://iith.ac.in/reports/" rel="noopener noreferrer">top 10 institutes</a>&nbsp;in India for Engineering&nbsp;<a href="https://www.nirfindia.org/2021/EngineeringRanking.html" rel="noopener noreferrer" target="_blank">according to NIRF</a>&nbsp;making it one of the most coveted schools for science and technology in the country.

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Journal of Thermal Analysis and Calorimetry

Solid-state synthesis and heat capacity measurements of ceramic compounds LiAlSiO4, LiAlSi2O6, LiAlSi3O 8, and LiAlSi4O10

Journal	Journal of Thermal Analysis and Calorimetry
ISSN	13886150