The present study was undertaken to develop a novel and easy practical approach for synthesis of cyclopentanone, a versatile industrial ingredient. Accordingly, ceria-zirconia based nano-oxide catalysts, namely, CexZr1-xO2 and CexZr1-xO2/M (M=SiO2 and Al2O3) were prepared and evaluated for the title reaction. The physicochemical characterization has been achieved using different techniques, namely, XRD, BET surface area, XPS, Raman, OSC, and HREM. The catalytic results revealed that CexZr1-xO2 based nano-oxides are promising heterogeneous catalysts for synthesis of cyclopentanone. Amongst, the CexZr1-xO2/Al2O3 catalyst exhibited ~100% conversion with 75% desired cyclopentanone product selectivity owing to its favorable physicochemical characteristics. © 2013 The Korean Society of Industrial and Engineering Chemistry.

Sudarsanam Putla

Department of Chemistry

L. Katta

G. Thrimurthulu

B.M. Reddy

Indian Institute of Technology Hyderabad (IITH) is a premier institute of science and technology established in 2008. IITH has been consistently ranked in the&nbsp;<a href="https://iith.ac.in/reports/" rel="noopener noreferrer">top 10 institutes</a>&nbsp;in India for Engineering&nbsp;<a href="https://www.nirfindia.org/2021/EngineeringRanking.html" rel="noopener noreferrer" target="_blank">according to NIRF</a>&nbsp;making it one of the most coveted schools for science and technology in the country.

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Journal	Journal of Industrial and Engineering Chemistry
ISSN	1226086X