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Synthesis and solid state structures of Chalcogenide compounds of Imidazolin-2-ylidene-1,1-Diphenyl-phosphinamine
K. Naktode, S. Das, A. Kundu, H.P. Nayek,
Published in Springer India
2016
Volume: 128
   
Issue: 3
Pages: 373 - 382
Abstract
We report the synthesis and solid state structures of 1,3-di-aryl-imidazolin-2-ylidine-1,1-diphenylphosphinamine [(aryl = mesityl (1a) and aryl = 2,6-diisopripyl (1b)] and their chalcogenide compounds 1, 3-di-aryl-imidazolin-2-ylidine- P,P-diphenylphosphinicamide (2a,b), 1,3-di-aryl-imidazolin-2-ylidine-P,P-diphenyl-phosphinothioicamide (3a,b) and 1,3-diaryl-imidazolin-2-ylidine- P,P-diphenyl-phosphinoselenoic-amide (4a,b). The compounds 1a,b were prepared in good yield by the reaction of 1,3-di-aryl-imidazolin-2-imine and chlorodiphenylphosphine in the presence of triethylamine in toluene. The reactions of 1a,b with elemental sulphur and selenium afforded the corresponding chalcogenide compounds 3a,b and 4a,b respectively. The corresponding oxo- derivative (2a,b) was obtained by reacting compound 1a,b with 30% aqueous hydrogen peroxide in THF. The molecular structures of 1a, 2a, 3a and 4a,b have been established by single crystal X-ray diffraction analyses. The molecular structures reveal that even C1-N1-P1 angle (124.62 °) in compound 1a is less obtuse compared to the corresponding C1-N1-Si1 angles (157.8 °) observed in related N-silylated 2-iminoimidazolines and trimethylsilyl iminophosphoranes. C1-N1-P1 angles are further widened in compounds 2a, 3a, and 4a,b due to the attachment of chalcogen atoms onto phosphorus atom. [Figure not available: see fulltext.] © 2016 Indian Academy of Sciences.
About the journal
JournalData powered by TypesetJournal of Chemical Sciences
PublisherData powered by TypesetSpringer India
ISSN09743626