The reaction of 1,3-bis(2,6-diisopropylphenyl)imidazolin-2-imine (Im DippNH) with trimethylsilylmethyllithium and anhydrous lutetium trichloride affords the imido complex [LuCl2(ImNDipp)(THF) 3] (1), which, on further reaction with dipotassium cyclooctatetraenide, K2(C8H8), leads to the half-sandwich cyclooctatetraenyl complex [(η8-C8H 8)Lu(ImNDipp)(THF)2]; both complexes contain very short Lu-N bond lengths, which are shorter than any previously reported Lu-N distances. © The Royal Society of Chemistry.

Tarun Kanti Panda

Department of Chemistry

S. Randoll

C.G. Hrib

P.G. Jones

T. Bannenberg

M. Tamm

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Chemical Communications

Syntheses and structures of mononuclear lutetium imido complexes with very short Lu-N bonds

Journal	Data powered by TypesetChemical Communications
Publisher	Data powered by TypesetRoyal Society of Chemistry
ISSN	13597345