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Sintering mechanisms of attrition milled titanium nano powder
, M.M. Godkhindi, K. Das, P.G. Mukunda, V.V. Dabhade, P. Ramakrishnan
Published in
2005
Volume: 20
   
Issue: 4
Pages: 827 - 836
Abstract
Detailed sintering studies have been carried out on attrition milled nanocrystalline titanium powder through isothermal dilatometry over a temperature range of 300 - 1250 °C along with microstructural and x-ray diffraction studies. The sintering behavior of attrition milled nanocrystalline titanium appears to be characterized by: (i) very low activation energies, (ii) high shrinkage anisotropy, (iii) very rapid grain growth in the beta range, and (iv) two kinds of densification processes, namely, intra-agglomerate and inter-agglomerate. Analysis of the kinetic data through sintering diagram approach indicates the operation of particle sliding and grain boundary rotation, type of mechanism in addition to the grain-boundary diffusion, and lattice diffusion as the dominant mass transport mechanisms. © 2005 Materials Research Society.
About the journal
JournalJournal of Materials Research
ISSN08842914